空的填充柱接到气相色谱仪gdx填充柱上柱前压力表有示数吗
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室内环境（TVOC）检测专用气相色谱仪配置表
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室内环境(TVOC)检测专用气相色谱仪配置表：&仪器名称型号及规格单位数量气相色谱仪主机+FID+填充系统+毛细系统台1主机+FID+填充系统主机+FID+毛细系统台2色谱工作站TVOC专用版 双通道台1空气发生器HS-3 0～3000ml/min&台1氢气发生器HS-300&0～310ml/min 99.999%台1氮气瓶高纯氮气99.999% 含减压阀套1热解吸仪解吸管活化仪&ATDS-6000D 自动解析仪-反吹-活化一体机TDS-3410A 解吸管活化及标样模拟采样一体机台台11分光光度计检测甲醛、氨气台1测氡仪连续测氡台1双气路大气采样器0.1～1.5L/min；连续可调定时：1～99min台1恒流 采样流量：0.4～0.6L/min台1恒流&工作流量范围：100～500ml/min台1空盒压力表压力表台1温湿度计测温湿度台1数显鼓风干燥箱350&350&350台1石英双重蒸馏水仪无氨水台1电子天平精度：0.1mg；称量范围：200g台1采样箱装吸收管、采样管等采样用品；配铝合金支架个1TVOC专用柱0.32mm*50m*1u支1苯专用柱3mm*2M支1Tenax吸附管200mg 50支/盒 （数量选配）盒1活性炭采样管50支/包 （数量选配）包1气泡吸收管10ml （数量选配）支1玻板吸收管10ml （数量选配）支1TVOC标液10、100、1000ug/ml套1苯系物标液2ml支1苯系物标气2L 5组份瓶1酚试剂5g瓶1甲醛溶液20ml 100mg/L或2ml 10.2mg/ml支1氨溶液20ml 500mg/L支1&河北睿达建工仪器设备有限公司生产销售：公路试验仪器，铁路试验仪器，混凝土试验仪器，万能材料试验机，压力试验机，水泥试验仪器，土工试验仪器，沥青试验仪器，砂浆试验仪器，防水卷材检测仪器，建筑节能检测仪器，测绘仪器，主体结构检测仪器，钢结构检测仪器，无损检测仪器，电线电缆检测仪器，管材管件检测仪器，陶瓷砖检测仪器，保温材料试验仪器，涂料试验仪器，土工合成材料检测仪器,室内环境检测仪器承揽各等级实验室的组建、配套服务，提供标准化的产品咨询、设备安装、使用培训、维修维护、升级改造等售前咨询、售中配合、售后保障服务！&本公司以优质的产品、专业的售后、超长的质保取得了国内外众多专业厂家的信任并建立了良好的长期合作关系，成功地在国内外各大科研院校、勘察设计、水电工程、路桥施工、检测监理、、建材生产等系统单位进行了推广，满足了用户各种不同的检测目的要求，提供了完善的检测仪器配置方案，得到了用户的高度认可！&我们将以踏实严谨、讲求效率的工作作风和真诚合作的态度来与用户建立良好的合作伙伴关系！以用户的宝贵经验提携我们，以我们优质的产品和专业服务为每一位用户创造价值! & & & & &&
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金牌企业：气相色谱仪毛细管柱气路压力表没示数？怎么回事呢？求化学、医学、物理、生物大神指教_百度知道
气相色谱仪毛细管柱气路压力表没示数？怎么回事呢？求化学、医学、物理、生物大神指教
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PGC2000过程气相色谱操作及服务手册(中文版)
操作及服务手册 过程气相色谱 PGC20002000-OSM C1: August 2002 注意 本手册包含的内容是ABB公司的专利资料并且只用于对本产品进行理解和操作规格如有变化将不再通知?2000 - 2002, ABB Inc.详情请联系: ABB Inc. 843 North Jefferson S树t P.O. Box 831 Lewisburg, WV 24901 总机: Telephone (304) 647-4358 传真Fax (304) 645-4236现场服务: Telephone (304) 340-0508 备件: Telephone (304) 647-1736 传真Fax (304) 647-1837请提供 销售订单号, 位号, 分析仪 零件号码和 序列号 目录Title 术语表 Page ............ G-1 SECTION 1. 介绍 产品描述 .................................................................................................................. 1-1 PGC2000 带光度检测器 .......................................................................... 1-2 空气吹扫系统 ........................................................................................................................ 1-3 系统类别 ........................................................................................................................... 1-3 规格表... 1-3 外形 ............ 1-3 安全区等级 ................................................................................................................. 1-3 电源 ................ 1-4 仪表空气 ... 1-4 分析检测器 ................................................................................................................... 1-4 等温分析炉 ............................................................................................................... 1-4 气体控制 (模拟).............................................................................................................. 1-5 气体控制 (数字) ............................................................................................................. 1-6 SECTION 2. 安装与启动 安装准备 ......................................................................................................... 2-1 安装工具与设备 ....................................................................................................... 2-1 管连接 ......................................................................................................................... 2-1 气体要求.......................................................................................................................... 2-2 标定样气.......................................................................................................................... 2-2 吹扫空气报警 ........................................................................................................ 2-2 液体进样阀 ...................................................................................................................... 2-2 设备就位 ....................................................................................................................... 2-3 连接 ......................................................................................................................... 2-3 管接 ...................................................................................................................... 2-3 分析仪空气 .............................................................................................................. 2-4 载气 .............................................................................................................. 2-4 样品 ....................................................................................................... .............. 2-4 氢气 ....................................................................................................... ... 2-4 排放 .......................................................................................................................... 2-4 电气 .................................................................................................................. 2-4 初次启动 ........................................................................................................... 2-5 设备和供货要求 .................................................................................................... 2-5 防范 ......................................................................................................................... 2-5 取样系统检查 ................................................................................................................ 2-6 色谱控制器预检 ............................................................................................................... 2-6 分析仪预检........................................................................................................................ 2-6 泄漏检测 .............................................................................................................. 2-7 协调色谱柱流量 ............................................................................................................... 2-8 手动操作阀 .............................................................................................................. 2-8 检查总色谱柱流量............................................................................................................. 2-9 检查分析流量调整 ...................................................................................................... 2-10 检查反吹流量 ................................................................................................................ 2-10 检查选择流量调整 ........................................................................................................ 2-12 iv 2000-OSM, C1 目录 (继续) Title Page 检查选择排放 ................................................................................................................... 2-12 设备启动 ........................................................................................................................ 2-13 初次上电 ............................................................................................................................. 2-13 核对色谱控制器操作 ........................................................................................................... 2-17 标定运行 ............................................................................................................................. 2-19 检查流路 .......................................................................................................................... 2-21 色谱输入输出板的设定 ....................................................................................................... 2-21 分析运行 ........................................................................................................................ 2-24 核对色谱图上的基线零位 .......................................................................................... 2-24 分析运行检查 ...................................................................................................................... 2-26 核对报告 ....................................................................................................... . 2-26 本底运行 ............................................................................................................................. 2-27 TCD 零位调整 (热导丝 TCD Only) .................................................................................... 2-28 停止分析 ..................................................................................................................... 2-29 连接色谱仪至VistaNET ..................................................................................... 2-29 初始启动 ............................................................................................................ 2-29 设定访问级 ..................................................................................................................... 2-31 用户清单 ....................................................................................................... 2-32 完成VistaNET连接 ............................................................................................. 2-34 SECTION 3. 操作 控制和指示 ............................................................................................................. 3-1 气相色谱控制器 (GCC) ........................................................................................... 3-1 调整压力表盘 ............................................................................................................ 3-2 隔离箱 ........................................................................................................................... 3-2 常规操作 ........................................................................................................................... 3-2 显示屏 ......................................................................................................... 3-2 检查标定 ......................................................................................................................... 3-3 检查流路 ............................................................................................................................. 3-4 分析操作 .......................................................................................................................... 3-5 报警 ........................................................................................................................ 3-6 色谱 .......................................................................................................3-7 显示一个色谱图 .............................................................................................................. 3-7 记录一个色谱图 .............................................................................................................. 3-7 停机步骤 ................................................................................................................ 3-8 命令树 .......................................................................................................... 3-9 SECTION 4. 技术描述 功能描述 ................................................................................................................ 4-1 检测器 ................................................................................................................. 4-2 介绍 .............................................................................................................. 4-2 火焰离子检测器 (FID) ........................................................................................................ 4-3 热导检测器 (TCD) ............................................................................................... 4-4 火焰光度检测器 (FPD) ................................................................................................... 4-5 柱间检测器 ......................................................................................................................... 4-5 顺序双检测器 ................................................................................................................. 4-6 并行双检测器 ............................................................................................................ 4-6 电路板 4-11 电源板 ......................................................................................................................... 4-11 iv 2000-OSM, C1 v 目录 (继续) Title Page 色谱输入输出板 ......................................................................................................................... 4-11 单板计算机板 (SBC) ................................................................................................ 4-11 直流电磁阀驱动板 ................................................................................................................. 4-11 面板 ............................................................................................................................. 4-11 FID 放大器 ........................................................................................................................... 4-12 TCD 放大器 ......................................................................................................................... 4-12 FPD 放大器和界面电路板 .................................................................................................. 4-12 数字温度控制底板 ..................................................................................................................... 4-12 交流温控电源板 ...................................................................................................................... 4-12 数字温度控制区域板................................................................................................................... 4-12 电子压力控制器多总线电路板.................................................................................................... 4-12 电子压力控制器板 ............................................................................................................... 4-12 电子压力控制器传感器板 .......................................................................................................... 4-13 本地通讯板 (选项) ................................................................................................................. 4-13 通讯板 (选项) ....................................................................................................... 4-13 模拟输出板 (选项) ........................................................................................................... 4-13 数字输入/输出板 (选项) ................................................................................................... 4-13 方法表 ....................................................................................................... 4-13 标定方法 .................................................................................................................... 4-13 准备一个方法表 ............................................................................................................... 4-15 编辑一个方法表 .................................................................................................................. 4-19 打印一个方法表 .................................................................................................................. 4-20 峰检测 ............................................................................................................................... 4-23 强制门 ........................................................................................................ 4-23 斜率检测: 介绍 ......................................................................................................... 4-23 斜率检测: 基本函数 ................................................................................................... 4-24 斜率检测: 辅助函数 ...................................................................................... 4-24 其他时序编码函数 .................................................................................................... 4-28 自动调零 ............................................................................................................... 4-28 流路步进 ........................................................................................................... 4-29 阀开/阀关 ................................................................................................................... 4-29 跟踪标识 ................................................................................................................. 4-29 报警时跳过下一时序码函数................................................................................................. 4-30 如果流路= 那末跳过下一时序函数 ............................................................................... 4-30 如果流路= 那末执行下一时序函数 ............................................................................... 4-30 压力检查.............................................................................................................................. 4-30 压力控制 ............................................................................................................................ 4-30 温度检查 ......................................................................................................................... 4-30 温度控制 ....................................................................................................................... 4-30 其他表和报告 ......................................................................................................... 4-30 观看/编辑表格 ................................................................................................................ 4-30 打印表格 ........................................................................................................................ 4-31 打印报告 ............................................................................................................................. 4-31 任意流路步进表 ...................................................................................................... 4-32 时刻表 .............................................................................................................................. 4-33 流路表 .......................................................................................................................... 4-34 原始数据报告...................................................................................................................... 4-35 常规报告 ....................................................................................................................... 4-36 简短报告 ........................................................................................................................... 4-36 标准标定报告 ............................................................................................................ 4-36 空气吹扫 .............................................................................................................................. 4-37 Y 和 Z 吹扫 ................................................................................................................... 4-37 2000-OSM, C1 v 目录 (继续) Title Page X 吹扫操作 .......................................................................................................................... 4-38 X 吹扫跨越操作 ................................................................................................................. 4-39 ............................................................................................................................. 4-40 E2PROM 存储表格至 E2PROM .......................................................................................................... 4-40 从E2PROM恢复表格 ......................................................................................................... 4-41 数字温度控制器 ............................................................................................ 4-42 物理描述 ........................................................................................................................ 4-42 操作器设定 ......................................................................................................................... 4-42 手动温度控制方式 ................................................................................................. 4-43 5区域命名和上下限表 ...................................................................................................... 4-44 设定开关 ....................................................................................................................... 4-46 温度控制表 .............................................................................................................. 4-48 温度控制检查表 ............................................................................................................... 4-49 控制器类型 ....................................................................................................................... 4-51 温度组态表 .................................................................................................... 4-52 程序注解 ........................................................................................................................ 4-53 报警 .................................................................................................................................. 4-54 电子压力控制选项 .................................................................................. 4-54 物理描述 ........................................................................................................................ 4-54 操作器设定.......................................................................................................................... 4-55 手动压力控制方式 ....................................................................................................... 4-55 压力组态表 .......................................................................................................... 4-57 设定开关 ....................................................................................................................... 4-59 压力控制表 .................................................................................................................... 4-60 压力检查表 ..................................................................................................................... 4-62 报警 .................................................................................................................................. 4-63 原始色谱图的存储和再生 ............................................................. 4-63 概论 ............................................................................................................................... 4-63 进入色谱图库 ......................................................................................... 4-64 检查可用的存储器 ............................................................................................................ 4-64 抹去 (释放) 色谱图 ....................................................................................... 4-65 存储色谱图 .................................................................................................................. 4-66 显示已存数据 .................................................................................................................... 4-67 再生已存色谱图 ............................................................................................ 4-68 远程色谱操作选项 .................................................................................................... 4-69 本地通讯设定 .................................................................................................................... 4-69 远程操作 ........................................................................................................................... 4-72 模拟输出选项 ................................................................................................................. 4-74 数字输入/输出选项 ................................................................................................................... 4-75 VistaNET 选项 ..................................................................................................................... 4-77 SECTION 5. 维护 预防性维护 ............................................................................................................... 5-1 气体钢瓶更换 ............................................................................................................... 5-1 清洁 ................................................................................................................................ 5-2 诊断测试 ............................................................................................................................. 5-2 只读存储器检查和.................................................................................................................. 5-2 色谱板 ....................................................................................................................... 5-4 数字输出 ........................................................................................................................ 5-4 趋势(模拟)输出...................................................................................................................... 5-6 vi 2000-OSM, C1 目录 (继续) Title Page 硬件设定 .................................................................................................................... 5-7 软件确认 .................................................................................................................. 5-8 起始步骤 .............................................................................................................................. 5-8 色谱板1输入表 ............................................................................................................. 5-9 色谱板1输出表 ......................................................................................................... 5-10 数字板1输入表 .............................................................................................................. 5-10 数字板1输出表 ............................................................................................................ 5-11 数字板2. .................................................................................................................... 5-12 色谱板2 .............................................................................................................................. 5-12 趋势和检测器 ...................................................................................................................... 5-13 BASIC 总体尺度 ................................................................................................................. 5-13 结束步骤 .......................................................................................................................... 5-14 SECTION 6. 故障处理 故障处理指导 ...................................................................................................... 6-1 基线问题 .......................................................................................................................... 6-1 基线或信号补偿 (TCD) ........................................................................................................ 6-1 周期性小漂移 ...................................................................................................................... 6-2 连续向上或向下漂移 ............................................................................................. 6-2 基线连续噪声 ............................................................................................................... 6-3 基线或信号补偿(FID) .......................................................................................................... 6-4 基线信号不规则噪声(FID) ................................................................................................ 6-4 基线或信号补偿(FPD) ........................................................................................................ 6-5 基线信号不规则噪声(FPD) .............................................................................................. 6-6 分析问题 .......................................................................................................................... 6-7 没有出峰 .............................................................................................................................. 6-7 复式取样 ............................................................................................................................... 6-8 不明来源的出峰 (神秘峰) ...................................................................... 6-9 不定的样品尺寸 .................................................................................................................. 6-10 不定的保留时间 ................................................................................................................ 6-10 个别峰的丢失 .................................................................................................. 6-11 峰倒置 .................................................................................................................... 6-11 色谱图超大或超量度 ........................................................................................... 6-12 检测器灵敏度降低 .......................................................................................................... 6-12 峰的识别 ........................................................................................................................ 6-13 分析流产 ............................................................................................ 6-13 温度控制硬件问题 ....................................................................... 6-14 温度探头开路 ................................................................................................................ 6-14 温度探头短路 ............................................................................................................ 6-15 等温箱加热器热电偶故障 ................................................................................ 6-15 温度控制 Micro #2 ......................................................................................................... 6-16 空气丢失 ........................................................................................................................... 6-16 可控硅故障 ........................................................................................................................ 6-17 升温速率(T-Rating) 冲突..................................................................................................... 6-18 排除跳线冲突 ..................................................................................................... 6-18 箱温大于升温率 .................................................................................. 6-19 合理性 ............................................................................................................................. 6-19 交流零点交叉点丢失........................................................................................................... 6-20 超温测试失败 ................................................................................................................. 6-20 控制箱内温度大于80摄氏度................................................................................................ 6-21 2000-OSM, C1 vii 目录 (继续) Title Page 设定点不接受 ................................................................................................................... 6-22 重新组态失败 ................................................................................................................... 6-22 不受控制 .. 6-22 加热器开路或短路............................................................................................................... 6-23 交流电源板保险管迸裂 ............................................................................................... 6-23 过低箱体温度 ................................................................................................................... 6-24 过高箱体温度 .................................................................................................................. 6-24 程序箱温不制冷或慢冷 ........................................................ 6-24 输出问题 ...................................................................................................................6-25 打印机不产生报告 ......................................................................................................... 6-25 趋势输出不正确 .......................................................................................... 6-25 数字电路板故障 .................................................................................................................. 6-25 无记录仪输出 ...................................................................................................................... 6-26 无Vista工作站通讯 ............................................................................................. 6-26 无分析仪键盘响应 ...................................................................................................... 6-26 本地通讯板的标识和可能的原因 .............................................................................. 6-26 火焰灭发光二极管点亮 ....................................................................................................... 6-27 火焰不燃(FID or FPD) .................................................................................................. 6-28 低载气压力硬件报警 ............................................................................................ 6-28 低样品流量硬件报警 ................................................................................................. 6-28 吹扫空气丢失 ...................................................................................................................... 6-29 流路没有选择...................................................................................................................... 6-29 分析仪没上电 (X-吹扫) ............................................................................................ 6-30 电子压力控制故障 ........................................................... 6-31 控制器问题 ................................................................................................................. 6-31 输入电源 ....................................................................................................................... 6-31 电源分配 ........................................................................................................................... 6-32 不当的显示器对比度............................................................................................................ 6-33 报警 .................................................................................................................................. 6-33 传感器活动 ................................................................................................................... 6-35 传感器保持 .................................................................................................................... 6-35 组分含量高 ........................................................................................................................ 6-36 组分含量低.......................................................................................................................... 6-36 时钟错误 .................................................................................................. 6-36 时间码功能(TCF)错误 .................................................................................................... 6-37 分析后错误 ......................................................................................................................... 6-37 通讯错误 .................................................................................................................... 6-38 压力板 ............................................................................................................................... 6-39 温度板 ......................................................................................................................... 6-40 原始色谱图存储 ........................................................................................................... 6-42 报警公共输出连接 ............................................................................................... 6-42 报警公共输出检查 ....................................................................................................... 6-43 SECTION 7. 测试步骤 TP 1: 载气, 稀释气, 和在用气的提供 ................................................................... 7-1 TP 2: 载气, 稀释气流量调整 .............................................................. 7-1 TP 3: 样品阀漏泄/色谱柱溢流 ....................................................................... 7-2 TP 4: 载气或稀释气调节器 ................................................................................ 7-3 TP 5: 热导检测器平衡 ........................................................................................................... 7-3 TP 6: 热导丝测试 .................................................................................................................. 7-4 2000-OSM, C1 ix 目录 (继续) Title Page TP 7: TCD 电气连接 .................................................................................................................... 7-5 TP 8: 色谱柱拖尾问题 ...................................................................................................... 7-6 TP 9: 基线周期温度控制器 (TCD) ....................................................... 7-7 TP 10: 基线周期载气调节器 ............................................................................ 7-7 TP 11: 基线周期流量控制器 ................................................................................ 7-7 TP 12: 共用气 .................................................................................................. 7-7 TP 13: 在用气体污染处理 ........................................................................ 7-7 TP 14: 燃烧气接触式清洁单元 ............................................................................... 7-8 TP 15: 同轴电缆 ........................................................................................................................ 7-8 TP 16: FID 灵敏度降低 ..................................................................................................... 7-9 TP 17: FID 不能点燃 ............................................................................................................... 7-10 TP 18: 确认火焰点燃 ........................................................................................ 7-11 TP 19: 样品阀的动力气源 ........................................................................................... 7-11 TP 20: 复式取样 ................................................................................................................ 7-12 TP 21: 可变的样品尺寸 ......................................................................................................... 7-13 TP 22: 开路温度探头 ............................................................................................ 7-14 TP 23: 短路温度探头 ..................................................................................... 7-14 TP 24: 箱体空气丢 ................................................................................................................ 7-15 TP 25: 等温箱超温探头开路 ............................................................... 7-16 TP 26: 区域输入探头开路 ................................................................................................. 7-17 TP 27: 加热器开路或短路 ................................................................................................. 7-18 TP 28: 交流电源保险丝开路 ......................................................................... 7-19 TP 29: FID 极化器电压测试 .......................................................................................... 7-19 TP 30: 点火后“火焰灭” LED仍然亮 ........................................... 7-21 TP 31: 检查温度表值 ......................................................................... 7-22 TP 32: 喷嘴或呼吸器堵塞 ............................................................................................... 7-27 TP 33: 峰的识别 .......................................................................................................... 7-28 TP 34: 检查方法表组态 .................................................................... 7-29 TP 35: 排放背压 ......................................................................................................... 7-33 TP 36: 打印机测试...................................................................................................................... 7-34 TP 37: 残余样品 ................................................................................................................ 7-34 TP 38: 趋势输出 ...................................................................................................................... 7-35 TP 39: 数字输入/输出板.............................................................................................................. 7-36 TP 40: 色谱工作站通讯试验 ................................................................... 7-37 TP 41: 过低载气压力 .................................................................................................... 7-37 TP 42: 过低样品压力硬件报警 ............................................................................ 7-38 TP 43: 程序温度箱冷却 ......................................................... 7-39 TP 44: 流路切换 ............................................................................................................. 7-40 TP 45: FPD 设定........................................................................................................................ 7-42 SECTION 8. 修理 更换加热器 .......................................................................................................................... 8-1 等温箱加热器 ............................................................................................... 8-1 样品阀加热器 ...................................................................................................................... 8-2 样品阀修理 ........................................................................................................................ 8-3 拆卸 ............................................................................................................................. 8-4 重装 ............................................................................................................................. 8-5 色谱柱安装或更换 ..................................................................................... 8-7 移去色谱柱 ..................................................................................................................8-7 填充柱安装 ............................................................................................................... 8-7 x 2000-OSM, C1 目录 (继续) Title Page 毛细管柱安装 ............................................................................................................. 8-8 切割毛细管柱 ................................................................................................................. 8-8 FID 修理 ................................................................................................................................... 8-9 FID 池的访问 .......................................................................................................................8-10 更换呼吸器 ................................................................................................................... 8-10 更换热电偶 .......................................................................................... 8-11 访问极化器和点火器 ................................................................................. 8-12 更换极化器 ................................................................................................................... 8-12 更换点火装置 ....................................................................................................... 8-13 最后检查检测器 ........................................................................................................................ 8-14 清洁FID喷嘴 ....................................................................................................................... 8-15 清洁收集器 ..................................................................................................................... 8-16 更换FID电缆 ................................................................................................. 8-16 热导丝修理 ...................................................................................................................... 8-17 热导检测器的访问...................................................................................................................... 8-18 移去热导丝 .................................................................................................................. 8-18 安装热导丝 .................................................................................................................... 8-19 热导丝检验 .......................................................................................................................... 8-19 连接热导丝 ................................................................................................................ 8-20 泄漏测试 ................................................................................................................................ 8-21 陶瓷热导丝(仅适用于CENELEC 和 CSA) ............................................................................ 8-21 电热调节式TCD修理 ................................................................................................................ 8-22 热导检测器的访问 ..................................................................................................................... 8-22 移去电热调节器 .............................................................................................................. 8-23 安装电热调节器 ................................................................................................................ 8-23 电热调节器检验 ....................................................................................................................... 8-24 连接电热调节器 ............................................................................................................ 8-25 泄漏测试 ................................................................................................................................ 8-25 FPD 修理 ................................................................................................................................ 8-26 更换光电倍增器 ......................................................................................... 8-26 更换光电倍增器O型圈 ............................................................................. 8-27 更换燃烧器模块O型圈 ............................................................................................................. 8-28 更换燃烧器模块 ............................................................................................... 8-28 甲烷化器/空气净化器修理 ................................................................................................ 8-29 移去甲烷化器/空气净化器组件 ............................................................................ 8-30 移出接触反应管 ......................................................................................................... 8-31 安装接触反应管 ........................................................................................................... 8-32 填充外壳 ....................................................................................................................... 8-32 安装甲烷化器/空气净化器组件 .............................................................................. 8-33 空气净化测试 ......................................................................................................................... 8-33 空气净化最终准备 ......................................................................................................... 8-34 修理载气盘(模拟) ........................................................................... 8-35 移去载气盘 .................................................................................................... 8-35 更换减压阀 ..................................................................................................................... 8-36 更换压力表 ......................................................................................................................... 8-37 安装载气盘 ...................................................................................................... 8-37 修理电子压力控制器(EPC) .................................................................................. 8-38 移去电子压力控制器 ............................................................................................. 8-38 安装电子压力控制器 ............................................................................................... 8-39 更换探头电路板 ................................................................................................................ 8-39 更换比例阀 ....................................................................................................... 8-40 2000-OSM, C1 xi 目录 (继续) Title Page 更换控制电路板 ............................................................................................................. 8-41 更换加热器 ...................................................................................................................... 8-42 标定电子压力控制器 ......................................................... 8-43 修理吹扫空气盘组件 ............................................................................... 8-45 移去吹扫空气盘 ........................................................................................................ 8-45 修理减压阀 ..................................................................................................................... 8-45 修理压力表 ......................................................................................................................... 8-46 安装吹扫空气盘 .......................................................................................................... 8-46 设置跳线 .............................................................................................. 8-46 色谱控制器底板.......................................................................................................................... 8-46 数字温度控制器底板................................................................................................................... 8-48 数字温度控制器(DTC)区域板 .................................................................................................... 8-49 交流电源板 .................................................................................................................... 8-50 前面盘电路板 ............................................................................................................................. 8-50 FID 放大器板 ........................................................................................................................... 8-51 热导丝TCD放大器板 ........................................................................................................... 8-51 电热调节器TCD 放大器界面板 ......................................................................................... 8-52 EPC 多总线板 .......................................................................................................................... 8-53 EPC 控制板 ............................................................................................................................ 8-54 色谱输入/输出板(色谱 输入/输出 PCB) (老式)................................................................................. 8-54 色谱输入/输出板 (新式) ........................................................................................................... 8-55 电源板 ......................................................................................................................... 8-56 VALCO 膜板阀修理 .................................................................................................. 8-56 移去阀 ........................................................................................................................ 8-56 修理阀 ......................................................................................................................... 8-57 重装阀 ...................................................................................................................... 8-58 VistaNET DEBUG监控............................................................................................................... 8-58 用途 .......... 8-58 确定连接 .................................................................................................................. 8-58 启动 ............ 8-59 信息显示 ......................................................................................................................... 8-60 菜单项 ..... 8-60 统计显示 ............................................................................................................................ 8-62 双空气净化器修理 .............................................................................................................. 8-65 移去双空气净化器 ...................................................................................... 8-66 移去空气净化管 .................................................................................................... 8-67 安装空气净化管 ...................................................................................................... 8-67 填充外壳 ....................................................................................................................... 8-67 安装双空气净化器 ........................................................................................ 8-68 空气净化测试 ......................................................................................................................... 8-69 空气净化最终准备 ......................................................................................................... 8-69 修理CP阀 ................................................................................................................. 8-70 更换滑块 ........................................................................................................................ 8-70 更换锲块 .................................................................................................................... 8-71 更换O型圈 .................................................................................................................... 8-71 SECTION 9. 更换部件 订购信息 ................................................................................................................... 9-1 设备标志 .................................................................................................................... 9-1 硬件组态标志 ................................................................................................ 9-1 xii 2000-OSM, C1 目录 (继续) Title Page 软件组态标志 ................................................................................................. 9-2 联系人 ........................................................................................................................ 9-2 色谱控制器 ........................................................................................................................ 9-3 前面门板后背 ....................................................................................................................... 9-3 卡笼 ................................................................................................................................ 9-3 色谱控制器(GCC)底盘 ................................................................................................................. 9-4 右侧门构件 ....................................................................................................... 9-4 吹扫空气盘 .................................................................................................................. 9-5 电子压力控制盘 ...................................................................................... 9-5 载气盘 ........................................................................................................................... 9-6 等温箱构件 ................................................................................................... 9-6 液体样品阀 .......................................................................................................................... 9-7 火焰离子检测器 ................................................................................................................. 9-8 热导丝型热导检测器 ................................................................................... 9-8 电热调节器式热导检测器 ............................................................................... 9-9 二位控制阀(M2CP 阀) ............................................................................................................. 9-9 781型甲烷化/空气净化系统 ..................................................................................... 9-10 805型甲烷化/空气净化系统 ..................................................................................... 9-10 VALCO 膜板阀 ................................................................................................................... 9-11 双空气净化系统 ................................................................................................................ 9-11 火焰光度检测器(FPD) ........................................................................................ 9-12 变压器和光电倍增器构件 ................................................................................ 9-12 燃烧器构件 .............................................................................................................. 9-12 程序温度箱 ............................................................................................. 9-13 带加热块的火焰离子检测器 ................................................................................... 9-14 带加热块的热导丝式热导检测器 ................................................................................. 9-14 SECTION 10. 色谱BASIC程序(VISTA BASIC) 介绍 ..................................................................................................................... 10-1 Using the Editor ........................................................................................................................ 10-1 Vista BASIC 行格式 ................................................................................................................ 10-2 字符集 ................................................................................................................ 10-2 常量 ...................................................................................................................... 10-3 变量 ....................................................................................................................... 10-3 数组 ........................................................................................................................... 10-4 表达式和运算符 ............................................................................................................. 10-4 字母表 ......................................................................................................................... 10-5 绝对值式 .......................................................................................................... 10-5 功能激活 ................................................................................................................ 10-5 活动流路命令 ...................................................................................................... 10-6 增加时间码命令 ....................................................................................................................... 10-6 报警功能 ............................................................................................................................. 10-6 分配流路函数 ................................................................................................................ 10-6 分配流路命令 ......................................................................................................... 10-7 BPRINT 语句 .............................................................................................................. 10-7 CHAIN 语句 ........................................................................................................................... 10-7 CHR$ 函数 ............................................................................................................................... 10-7 清除命令 .......................................................................................................................... 10-7 时钟错误报警函数 .................................................................................................. 10-7 2000-OSM, C1 xiii 目录 (继续) Title Page 公用浮点数组 ....................................................................................................... 10-8 公用字符串组 ............................................................}
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室内环境(TVOC)检测专用气相色谱仪配置表：&仪器名称型号及规格单位数量气相色谱仪主机+FID+填充系统+毛细系统台1主机+FID+填充系统主机+FID+毛细系统台2色谱工作站TVOC专用版 双通道台1空气发生器HS-3 0～3000ml/min&台1氢气发生器HS-300&0～310ml/min 99.999%台1氮气瓶高纯氮气99.999% 含减压阀套1热解吸仪解吸管活化仪&ATDS-6000D 自动解析仪-反吹-活化一体机TDS-3410A 解吸管活化及标样模拟采样一体机台台11分光光度计检测甲醛、氨气台1测氡仪连续测氡台1双气路大气采样器0.1～1.5L/min；连续可调定时：1～99min台1恒流 采样流量：0.4～0.6L/min台1恒流&工作流量范围：100～500ml/min台1空盒压力表压力表台1温湿度计测温湿度台1数显鼓风干燥箱350&350&350台1石英双重蒸馏水仪无氨水台1电子天平精度：0.1mg；称量范围：200g台1采样箱装吸收管、采样管等采样用品；配铝合金支架个1TVOC专用柱0.32mm*50m*1u支1苯专用柱3mm*2M支1Tenax吸附管200mg 50支/盒 （数量选配）盒1活性炭采样管50支/包 （数量选配）包1气泡吸收管10ml （数量选配）支1玻板吸收管10ml （数量选配）支1TVOC标液10、100、1000ug/ml套1苯系物标液2ml支1苯系物标气2L 5组份瓶1酚试剂5g瓶1甲醛溶液20ml 100mg/L或2ml 10.2mg/ml支1氨溶液20ml 500mg/L支1&河北睿达建工仪器设备有限公司生产销售：公路试验仪器，铁路试验仪器，混凝土试验仪器，万能材料试验机，压力试验机，水泥试验仪器，土工试验仪器，沥青试验仪器，砂浆试验仪器，防水卷材检测仪器，建筑节能检测仪器，测绘仪器，主体结构检测仪器，钢结构检测仪器，无损检测仪器，电线电缆检测仪器，管材管件检测仪器，陶瓷砖检测仪器，保温材料试验仪器，涂料试验仪器，土工合成材料检测仪器,室内环境检测仪器承揽各等级实验室的组建、配套服务，提供标准化的产品咨询、设备安装、使用培训、维修维护、升级改造等售前咨询、售中配合、售后保障服务！&本公司以优质的产品、专业的售后、超长的质保取得了国内外众多专业厂家的信任并建立了良好的长期合作关系，成功地在国内外各大科研院校、勘察设计、水电工程、路桥施工、检测监理、、建材生产等系统单位进行了推广，满足了用户各种不同的检测目的要求，提供了完善的检测仪器配置方案，得到了用户的高度认可！&我们将以踏实严谨、讲求效率的工作作风和真诚合作的态度来与用户建立良好的合作伙伴关系！以用户的宝贵经验提携我们，以我们优质的产品和专业服务为每一位用户创造价值! & & & & &&
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PGC2000过程气相色谱操作及服务手册(中文版)
操作及服务手册 过程气相色谱 PGC20002000-OSM C1: August 2002 注意 本手册包含的内容是ABB公司的专利资料并且只用于对本产品进行理解和操作规格如有变化将不再通知?2000 - 2002, ABB Inc.详情请联系: ABB Inc. 843 North Jefferson S树t P.O. Box 831 Lewisburg, WV 24901 总机: Telephone (304) 647-4358 传真Fax (304) 645-4236现场服务: Telephone (304) 340-0508 备件: Telephone (304) 647-1736 传真Fax (304) 647-1837请提供 销售订单号, 位号, 分析仪 零件号码和 序列号 目录Title 术语表 Page ............ G-1 SECTION 1. 介绍 产品描述 .................................................................................................................. 1-1 PGC2000 带光度检测器 .......................................................................... 1-2 空气吹扫系统 ........................................................................................................................ 1-3 系统类别 ........................................................................................................................... 1-3 规格表... 1-3 外形 ............ 1-3 安全区等级 ................................................................................................................. 1-3 电源 ................ 1-4 仪表空气 ... 1-4 分析检测器 ................................................................................................................... 1-4 等温分析炉 ............................................................................................................... 1-4 气体控制 (模拟).............................................................................................................. 1-5 气体控制 (数字) ............................................................................................................. 1-6 SECTION 2. 安装与启动 安装准备 ......................................................................................................... 2-1 安装工具与设备 ....................................................................................................... 2-1 管连接 ......................................................................................................................... 2-1 气体要求.......................................................................................................................... 2-2 标定样气.......................................................................................................................... 2-2 吹扫空气报警 ........................................................................................................ 2-2 液体进样阀 ...................................................................................................................... 2-2 设备就位 ....................................................................................................................... 2-3 连接 ......................................................................................................................... 2-3 管接 ...................................................................................................................... 2-3 分析仪空气 .............................................................................................................. 2-4 载气 .............................................................................................................. 2-4 样品 ....................................................................................................... .............. 2-4 氢气 ....................................................................................................... ... 2-4 排放 .......................................................................................................................... 2-4 电气 .................................................................................................................. 2-4 初次启动 ........................................................................................................... 2-5 设备和供货要求 .................................................................................................... 2-5 防范 ......................................................................................................................... 2-5 取样系统检查 ................................................................................................................ 2-6 色谱控制器预检 ............................................................................................................... 2-6 分析仪预检........................................................................................................................ 2-6 泄漏检测 .............................................................................................................. 2-7 协调色谱柱流量 ............................................................................................................... 2-8 手动操作阀 .............................................................................................................. 2-8 检查总色谱柱流量............................................................................................................. 2-9 检查分析流量调整 ...................................................................................................... 2-10 检查反吹流量 ................................................................................................................ 2-10 检查选择流量调整 ........................................................................................................ 2-12 iv 2000-OSM, C1 目录 (继续) Title Page 检查选择排放 ................................................................................................................... 2-12 设备启动 ........................................................................................................................ 2-13 初次上电 ............................................................................................................................. 2-13 核对色谱控制器操作 ........................................................................................................... 2-17 标定运行 ............................................................................................................................. 2-19 检查流路 .......................................................................................................................... 2-21 色谱输入输出板的设定 ....................................................................................................... 2-21 分析运行 ........................................................................................................................ 2-24 核对色谱图上的基线零位 .......................................................................................... 2-24 分析运行检查 ...................................................................................................................... 2-26 核对报告 ....................................................................................................... . 2-26 本底运行 ............................................................................................................................. 2-27 TCD 零位调整 (热导丝 TCD Only) .................................................................................... 2-28 停止分析 ..................................................................................................................... 2-29 连接色谱仪至VistaNET ..................................................................................... 2-29 初始启动 ............................................................................................................ 2-29 设定访问级 ..................................................................................................................... 2-31 用户清单 ....................................................................................................... 2-32 完成VistaNET连接 ............................................................................................. 2-34 SECTION 3. 操作 控制和指示 ............................................................................................................. 3-1 气相色谱控制器 (GCC) ........................................................................................... 3-1 调整压力表盘 ............................................................................................................ 3-2 隔离箱 ........................................................................................................................... 3-2 常规操作 ........................................................................................................................... 3-2 显示屏 ......................................................................................................... 3-2 检查标定 ......................................................................................................................... 3-3 检查流路 ............................................................................................................................. 3-4 分析操作 .......................................................................................................................... 3-5 报警 ........................................................................................................................ 3-6 色谱 .......................................................................................................3-7 显示一个色谱图 .............................................................................................................. 3-7 记录一个色谱图 .............................................................................................................. 3-7 停机步骤 ................................................................................................................ 3-8 命令树 .......................................................................................................... 3-9 SECTION 4. 技术描述 功能描述 ................................................................................................................ 4-1 检测器 ................................................................................................................. 4-2 介绍 .............................................................................................................. 4-2 火焰离子检测器 (FID) ........................................................................................................ 4-3 热导检测器 (TCD) ............................................................................................... 4-4 火焰光度检测器 (FPD) ................................................................................................... 4-5 柱间检测器 ......................................................................................................................... 4-5 顺序双检测器 ................................................................................................................. 4-6 并行双检测器 ............................................................................................................ 4-6 电路板 4-11 电源板 ......................................................................................................................... 4-11 iv 2000-OSM, C1 v 目录 (继续) Title Page 色谱输入输出板 ......................................................................................................................... 4-11 单板计算机板 (SBC) ................................................................................................ 4-11 直流电磁阀驱动板 ................................................................................................................. 4-11 面板 ............................................................................................................................. 4-11 FID 放大器 ........................................................................................................................... 4-12 TCD 放大器 ......................................................................................................................... 4-12 FPD 放大器和界面电路板 .................................................................................................. 4-12 数字温度控制底板 ..................................................................................................................... 4-12 交流温控电源板 ...................................................................................................................... 4-12 数字温度控制区域板................................................................................................................... 4-12 电子压力控制器多总线电路板.................................................................................................... 4-12 电子压力控制器板 ............................................................................................................... 4-12 电子压力控制器传感器板 .......................................................................................................... 4-13 本地通讯板 (选项) ................................................................................................................. 4-13 通讯板 (选项) ....................................................................................................... 4-13 模拟输出板 (选项) ........................................................................................................... 4-13 数字输入/输出板 (选项) ................................................................................................... 4-13 方法表 ....................................................................................................... 4-13 标定方法 .................................................................................................................... 4-13 准备一个方法表 ............................................................................................................... 4-15 编辑一个方法表 .................................................................................................................. 4-19 打印一个方法表 .................................................................................................................. 4-20 峰检测 ............................................................................................................................... 4-23 强制门 ........................................................................................................ 4-23 斜率检测: 介绍 ......................................................................................................... 4-23 斜率检测: 基本函数 ................................................................................................... 4-24 斜率检测: 辅助函数 ...................................................................................... 4-24 其他时序编码函数 .................................................................................................... 4-28 自动调零 ............................................................................................................... 4-28 流路步进 ........................................................................................................... 4-29 阀开/阀关 ................................................................................................................... 4-29 跟踪标识 ................................................................................................................. 4-29 报警时跳过下一时序码函数................................................................................................. 4-30 如果流路= 那末跳过下一时序函数 ............................................................................... 4-30 如果流路= 那末执行下一时序函数 ............................................................................... 4-30 压力检查.............................................................................................................................. 4-30 压力控制 ............................................................................................................................ 4-30 温度检查 ......................................................................................................................... 4-30 温度控制 ....................................................................................................................... 4-30 其他表和报告 ......................................................................................................... 4-30 观看/编辑表格 ................................................................................................................ 4-30 打印表格 ........................................................................................................................ 4-31 打印报告 ............................................................................................................................. 4-31 任意流路步进表 ...................................................................................................... 4-32 时刻表 .............................................................................................................................. 4-33 流路表 .......................................................................................................................... 4-34 原始数据报告...................................................................................................................... 4-35 常规报告 ....................................................................................................................... 4-36 简短报告 ........................................................................................................................... 4-36 标准标定报告 ............................................................................................................ 4-36 空气吹扫 .............................................................................................................................. 4-37 Y 和 Z 吹扫 ................................................................................................................... 4-37 2000-OSM, C1 v 目录 (继续) Title Page X 吹扫操作 .......................................................................................................................... 4-38 X 吹扫跨越操作 ................................................................................................................. 4-39 ............................................................................................................................. 4-40 E2PROM 存储表格至 E2PROM .......................................................................................................... 4-40 从E2PROM恢复表格 ......................................................................................................... 4-41 数字温度控制器 ............................................................................................ 4-42 物理描述 ........................................................................................................................ 4-42 操作器设定 ......................................................................................................................... 4-42 手动温度控制方式 ................................................................................................. 4-43 5区域命名和上下限表 ...................................................................................................... 4-44 设定开关 ....................................................................................................................... 4-46 温度控制表 .............................................................................................................. 4-48 温度控制检查表 ............................................................................................................... 4-49 控制器类型 ....................................................................................................................... 4-51 温度组态表 .................................................................................................... 4-52 程序注解 ........................................................................................................................ 4-53 报警 .................................................................................................................................. 4-54 电子压力控制选项 .................................................................................. 4-54 物理描述 ........................................................................................................................ 4-54 操作器设定.......................................................................................................................... 4-55 手动压力控制方式 ....................................................................................................... 4-55 压力组态表 .......................................................................................................... 4-57 设定开关 ....................................................................................................................... 4-59 压力控制表 .................................................................................................................... 4-60 压力检查表 ..................................................................................................................... 4-62 报警 .................................................................................................................................. 4-63 原始色谱图的存储和再生 ............................................................. 4-63 概论 ............................................................................................................................... 4-63 进入色谱图库 ......................................................................................... 4-64 检查可用的存储器 ............................................................................................................ 4-64 抹去 (释放) 色谱图 ....................................................................................... 4-65 存储色谱图 .................................................................................................................. 4-66 显示已存数据 .................................................................................................................... 4-67 再生已存色谱图 ............................................................................................ 4-68 远程色谱操作选项 .................................................................................................... 4-69 本地通讯设定 .................................................................................................................... 4-69 远程操作 ........................................................................................................................... 4-72 模拟输出选项 ................................................................................................................. 4-74 数字输入/输出选项 ................................................................................................................... 4-75 VistaNET 选项 ..................................................................................................................... 4-77 SECTION 5. 维护 预防性维护 ............................................................................................................... 5-1 气体钢瓶更换 ............................................................................................................... 5-1 清洁 ................................................................................................................................ 5-2 诊断测试 ............................................................................................................................. 5-2 只读存储器检查和.................................................................................................................. 5-2 色谱板 ....................................................................................................................... 5-4 数字输出 ........................................................................................................................ 5-4 趋势(模拟)输出...................................................................................................................... 5-6 vi 2000-OSM, C1 目录 (继续) Title Page 硬件设定 .................................................................................................................... 5-7 软件确认 .................................................................................................................. 5-8 起始步骤 .............................................................................................................................. 5-8 色谱板1输入表 ............................................................................................................. 5-9 色谱板1输出表 ......................................................................................................... 5-10 数字板1输入表 .............................................................................................................. 5-10 数字板1输出表 ............................................................................................................ 5-11 数字板2. .................................................................................................................... 5-12 色谱板2 .............................................................................................................................. 5-12 趋势和检测器 ...................................................................................................................... 5-13 BASIC 总体尺度 ................................................................................................................. 5-13 结束步骤 .......................................................................................................................... 5-14 SECTION 6. 故障处理 故障处理指导 ...................................................................................................... 6-1 基线问题 .......................................................................................................................... 6-1 基线或信号补偿 (TCD) ........................................................................................................ 6-1 周期性小漂移 ...................................................................................................................... 6-2 连续向上或向下漂移 ............................................................................................. 6-2 基线连续噪声 ............................................................................................................... 6-3 基线或信号补偿(FID) .......................................................................................................... 6-4 基线信号不规则噪声(FID) ................................................................................................ 6-4 基线或信号补偿(FPD) ........................................................................................................ 6-5 基线信号不规则噪声(FPD) .............................................................................................. 6-6 分析问题 .......................................................................................................................... 6-7 没有出峰 .............................................................................................................................. 6-7 复式取样 ............................................................................................................................... 6-8 不明来源的出峰 (神秘峰) ...................................................................... 6-9 不定的样品尺寸 .................................................................................................................. 6-10 不定的保留时间 ................................................................................................................ 6-10 个别峰的丢失 .................................................................................................. 6-11 峰倒置 .................................................................................................................... 6-11 色谱图超大或超量度 ........................................................................................... 6-12 检测器灵敏度降低 .......................................................................................................... 6-12 峰的识别 ........................................................................................................................ 6-13 分析流产 ............................................................................................ 6-13 温度控制硬件问题 ....................................................................... 6-14 温度探头开路 ................................................................................................................ 6-14 温度探头短路 ............................................................................................................ 6-15 等温箱加热器热电偶故障 ................................................................................ 6-15 温度控制 Micro #2 ......................................................................................................... 6-16 空气丢失 ........................................................................................................................... 6-16 可控硅故障 ........................................................................................................................ 6-17 升温速率(T-Rating) 冲突..................................................................................................... 6-18 排除跳线冲突 ..................................................................................................... 6-18 箱温大于升温率 .................................................................................. 6-19 合理性 ............................................................................................................................. 6-19 交流零点交叉点丢失........................................................................................................... 6-20 超温测试失败 ................................................................................................................. 6-20 控制箱内温度大于80摄氏度................................................................................................ 6-21 2000-OSM, C1 vii 目录 (继续) Title Page 设定点不接受 ................................................................................................................... 6-22 重新组态失败 ................................................................................................................... 6-22 不受控制 .. 6-22 加热器开路或短路............................................................................................................... 6-23 交流电源板保险管迸裂 ............................................................................................... 6-23 过低箱体温度 ................................................................................................................... 6-24 过高箱体温度 .................................................................................................................. 6-24 程序箱温不制冷或慢冷 ........................................................ 6-24 输出问题 ...................................................................................................................6-25 打印机不产生报告 ......................................................................................................... 6-25 趋势输出不正确 .......................................................................................... 6-25 数字电路板故障 .................................................................................................................. 6-25 无记录仪输出 ...................................................................................................................... 6-26 无Vista工作站通讯 ............................................................................................. 6-26 无分析仪键盘响应 ...................................................................................................... 6-26 本地通讯板的标识和可能的原因 .............................................................................. 6-26 火焰灭发光二极管点亮 ....................................................................................................... 6-27 火焰不燃(FID or FPD) .................................................................................................. 6-28 低载气压力硬件报警 ............................................................................................ 6-28 低样品流量硬件报警 ................................................................................................. 6-28 吹扫空气丢失 ...................................................................................................................... 6-29 流路没有选择...................................................................................................................... 6-29 分析仪没上电 (X-吹扫) ............................................................................................ 6-30 电子压力控制故障 ........................................................... 6-31 控制器问题 ................................................................................................................. 6-31 输入电源 ....................................................................................................................... 6-31 电源分配 ........................................................................................................................... 6-32 不当的显示器对比度............................................................................................................ 6-33 报警 .................................................................................................................................. 6-33 传感器活动 ................................................................................................................... 6-35 传感器保持 .................................................................................................................... 6-35 组分含量高 ........................................................................................................................ 6-36 组分含量低.......................................................................................................................... 6-36 时钟错误 .................................................................................................. 6-36 时间码功能(TCF)错误 .................................................................................................... 6-37 分析后错误 ......................................................................................................................... 6-37 通讯错误 .................................................................................................................... 6-38 压力板 ............................................................................................................................... 6-39 温度板 ......................................................................................................................... 6-40 原始色谱图存储 ........................................................................................................... 6-42 报警公共输出连接 ............................................................................................... 6-42 报警公共输出检查 ....................................................................................................... 6-43 SECTION 7. 测试步骤 TP 1: 载气, 稀释气, 和在用气的提供 ................................................................... 7-1 TP 2: 载气, 稀释气流量调整 .............................................................. 7-1 TP 3: 样品阀漏泄/色谱柱溢流 ....................................................................... 7-2 TP 4: 载气或稀释气调节器 ................................................................................ 7-3 TP 5: 热导检测器平衡 ........................................................................................................... 7-3 TP 6: 热导丝测试 .................................................................................................................. 7-4 2000-OSM, C1 ix 目录 (继续) Title Page TP 7: TCD 电气连接 .................................................................................................................... 7-5 TP 8: 色谱柱拖尾问题 ...................................................................................................... 7-6 TP 9: 基线周期温度控制器 (TCD) ....................................................... 7-7 TP 10: 基线周期载气调节器 ............................................................................ 7-7 TP 11: 基线周期流量控制器 ................................................................................ 7-7 TP 12: 共用气 .................................................................................................. 7-7 TP 13: 在用气体污染处理 ........................................................................ 7-7 TP 14: 燃烧气接触式清洁单元 ............................................................................... 7-8 TP 15: 同轴电缆 ........................................................................................................................ 7-8 TP 16: FID 灵敏度降低 ..................................................................................................... 7-9 TP 17: FID 不能点燃 ............................................................................................................... 7-10 TP 18: 确认火焰点燃 ........................................................................................ 7-11 TP 19: 样品阀的动力气源 ........................................................................................... 7-11 TP 20: 复式取样 ................................................................................................................ 7-12 TP 21: 可变的样品尺寸 ......................................................................................................... 7-13 TP 22: 开路温度探头 ............................................................................................ 7-14 TP 23: 短路温度探头 ..................................................................................... 7-14 TP 24: 箱体空气丢 ................................................................................................................ 7-15 TP 25: 等温箱超温探头开路 ............................................................... 7-16 TP 26: 区域输入探头开路 ................................................................................................. 7-17 TP 27: 加热器开路或短路 ................................................................................................. 7-18 TP 28: 交流电源保险丝开路 ......................................................................... 7-19 TP 29: FID 极化器电压测试 .......................................................................................... 7-19 TP 30: 点火后“火焰灭” LED仍然亮 ........................................... 7-21 TP 31: 检查温度表值 ......................................................................... 7-22 TP 32: 喷嘴或呼吸器堵塞 ............................................................................................... 7-27 TP 33: 峰的识别 .......................................................................................................... 7-28 TP 34: 检查方法表组态 .................................................................... 7-29 TP 35: 排放背压 ......................................................................................................... 7-33 TP 36: 打印机测试...................................................................................................................... 7-34 TP 37: 残余样品 ................................................................................................................ 7-34 TP 38: 趋势输出 ...................................................................................................................... 7-35 TP 39: 数字输入/输出板.............................................................................................................. 7-36 TP 40: 色谱工作站通讯试验 ................................................................... 7-37 TP 41: 过低载气压力 .................................................................................................... 7-37 TP 42: 过低样品压力硬件报警 ............................................................................ 7-38 TP 43: 程序温度箱冷却 ......................................................... 7-39 TP 44: 流路切换 ............................................................................................................. 7-40 TP 45: FPD 设定........................................................................................................................ 7-42 SECTION 8. 修理 更换加热器 .......................................................................................................................... 8-1 等温箱加热器 ............................................................................................... 8-1 样品阀加热器 ...................................................................................................................... 8-2 样品阀修理 ........................................................................................................................ 8-3 拆卸 ............................................................................................................................. 8-4 重装 ............................................................................................................................. 8-5 色谱柱安装或更换 ..................................................................................... 8-7 移去色谱柱 ..................................................................................................................8-7 填充柱安装 ............................................................................................................... 8-7 x 2000-OSM, C1 目录 (继续) Title Page 毛细管柱安装 ............................................................................................................. 8-8 切割毛细管柱 ................................................................................................................. 8-8 FID 修理 ................................................................................................................................... 8-9 FID 池的访问 .......................................................................................................................8-10 更换呼吸器 ................................................................................................................... 8-10 更换热电偶 .......................................................................................... 8-11 访问极化器和点火器 ................................................................................. 8-12 更换极化器 ................................................................................................................... 8-12 更换点火装置 ....................................................................................................... 8-13 最后检查检测器 ........................................................................................................................ 8-14 清洁FID喷嘴 ....................................................................................................................... 8-15 清洁收集器 ..................................................................................................................... 8-16 更换FID电缆 ................................................................................................. 8-16 热导丝修理 ...................................................................................................................... 8-17 热导检测器的访问...................................................................................................................... 8-18 移去热导丝 .................................................................................................................. 8-18 安装热导丝 .................................................................................................................... 8-19 热导丝检验 .......................................................................................................................... 8-19 连接热导丝 ................................................................................................................ 8-20 泄漏测试 ................................................................................................................................ 8-21 陶瓷热导丝(仅适用于CENELEC 和 CSA) ............................................................................ 8-21 电热调节式TCD修理 ................................................................................................................ 8-22 热导检测器的访问 ..................................................................................................................... 8-22 移去电热调节器 .............................................................................................................. 8-23 安装电热调节器 ................................................................................................................ 8-23 电热调节器检验 ....................................................................................................................... 8-24 连接电热调节器 ............................................................................................................ 8-25 泄漏测试 ................................................................................................................................ 8-25 FPD 修理 ................................................................................................................................ 8-26 更换光电倍增器 ......................................................................................... 8-26 更换光电倍增器O型圈 ............................................................................. 8-27 更换燃烧器模块O型圈 ............................................................................................................. 8-28 更换燃烧器模块 ............................................................................................... 8-28 甲烷化器/空气净化器修理 ................................................................................................ 8-29 移去甲烷化器/空气净化器组件 ............................................................................ 8-30 移出接触反应管 ......................................................................................................... 8-31 安装接触反应管 ........................................................................................................... 8-32 填充外壳 ....................................................................................................................... 8-32 安装甲烷化器/空气净化器组件 .............................................................................. 8-33 空气净化测试 ......................................................................................................................... 8-33 空气净化最终准备 ......................................................................................................... 8-34 修理载气盘(模拟) ........................................................................... 8-35 移去载气盘 .................................................................................................... 8-35 更换减压阀 ..................................................................................................................... 8-36 更换压力表 ......................................................................................................................... 8-37 安装载气盘 ...................................................................................................... 8-37 修理电子压力控制器(EPC) .................................................................................. 8-38 移去电子压力控制器 ............................................................................................. 8-38 安装电子压力控制器 ............................................................................................... 8-39 更换探头电路板 ................................................................................................................ 8-39 更换比例阀 ....................................................................................................... 8-40 2000-OSM, C1 xi 目录 (继续) Title Page 更换控制电路板 ............................................................................................................. 8-41 更换加热器 ...................................................................................................................... 8-42 标定电子压力控制器 ......................................................... 8-43 修理吹扫空气盘组件 ............................................................................... 8-45 移去吹扫空气盘 ........................................................................................................ 8-45 修理减压阀 ..................................................................................................................... 8-45 修理压力表 ......................................................................................................................... 8-46 安装吹扫空气盘 .......................................................................................................... 8-46 设置跳线 .............................................................................................. 8-46 色谱控制器底板.......................................................................................................................... 8-46 数字温度控制器底板................................................................................................................... 8-48 数字温度控制器(DTC)区域板 .................................................................................................... 8-49 交流电源板 .................................................................................................................... 8-50 前面盘电路板 ............................................................................................................................. 8-50 FID 放大器板 ........................................................................................................................... 8-51 热导丝TCD放大器板 ........................................................................................................... 8-51 电热调节器TCD 放大器界面板 ......................................................................................... 8-52 EPC 多总线板 .......................................................................................................................... 8-53 EPC 控制板 ............................................................................................................................ 8-54 色谱输入/输出板(色谱 输入/输出 PCB) (老式)................................................................................. 8-54 色谱输入/输出板 (新式) ........................................................................................................... 8-55 电源板 ......................................................................................................................... 8-56 VALCO 膜板阀修理 .................................................................................................. 8-56 移去阀 ........................................................................................................................ 8-56 修理阀 ......................................................................................................................... 8-57 重装阀 ...................................................................................................................... 8-58 VistaNET DEBUG监控............................................................................................................... 8-58 用途 .......... 8-58 确定连接 .................................................................................................................. 8-58 启动 ............ 8-59 信息显示 ......................................................................................................................... 8-60 菜单项 ..... 8-60 统计显示 ............................................................................................................................ 8-62 双空气净化器修理 .............................................................................................................. 8-65 移去双空气净化器 ...................................................................................... 8-66 移去空气净化管 .................................................................................................... 8-67 安装空气净化管 ...................................................................................................... 8-67 填充外壳 ....................................................................................................................... 8-67 安装双空气净化器 ........................................................................................ 8-68 空气净化测试 ......................................................................................................................... 8-69 空气净化最终准备 ......................................................................................................... 8-69 修理CP阀 ................................................................................................................. 8-70 更换滑块 ........................................................................................................................ 8-70 更换锲块 .................................................................................................................... 8-71 更换O型圈 .................................................................................................................... 8-71 SECTION 9. 更换部件 订购信息 ................................................................................................................... 9-1 设备标志 .................................................................................................................... 9-1 硬件组态标志 ................................................................................................ 9-1 xii 2000-OSM, C1 目录 (继续) Title Page 软件组态标志 ................................................................................................. 9-2 联系人 ........................................................................................................................ 9-2 色谱控制器 ........................................................................................................................ 9-3 前面门板后背 ....................................................................................................................... 9-3 卡笼 ................................................................................................................................ 9-3 色谱控制器(GCC)底盘 ................................................................................................................. 9-4 右侧门构件 ....................................................................................................... 9-4 吹扫空气盘 .................................................................................................................. 9-5 电子压力控制盘 ...................................................................................... 9-5 载气盘 ........................................................................................................................... 9-6 等温箱构件 ................................................................................................... 9-6 液体样品阀 .......................................................................................................................... 9-7 火焰离子检测器 ................................................................................................................. 9-8 热导丝型热导检测器 ................................................................................... 9-8 电热调节器式热导检测器 ............................................................................... 9-9 二位控制阀(M2CP 阀) ............................................................................................................. 9-9 781型甲烷化/空气净化系统 ..................................................................................... 9-10 805型甲烷化/空气净化系统 ..................................................................................... 9-10 VALCO 膜板阀 ................................................................................................................... 9-11 双空气净化系统 ................................................................................................................ 9-11 火焰光度检测器(FPD) ........................................................................................ 9-12 变压器和光电倍增器构件 ................................................................................ 9-12 燃烧器构件 .............................................................................................................. 9-12 程序温度箱 ............................................................................................. 9-13 带加热块的火焰离子检测器 ................................................................................... 9-14 带加热块的热导丝式热导检测器 ................................................................................. 9-14 SECTION 10. 色谱BASIC程序(VISTA BASIC) 介绍 ..................................................................................................................... 10-1 Using the Editor ........................................................................................................................ 10-1 Vista BASIC 行格式 ................................................................................................................ 10-2 字符集 ................................................................................................................ 10-2 常量 ...................................................................................................................... 10-3 变量 ....................................................................................................................... 10-3 数组 ........................................................................................................................... 10-4 表达式和运算符 ............................................................................................................. 10-4 字母表 ......................................................................................................................... 10-5 绝对值式 .......................................................................................................... 10-5 功能激活 ................................................................................................................ 10-5 活动流路命令 ...................................................................................................... 10-6 增加时间码命令 ....................................................................................................................... 10-6 报警功能 ............................................................................................................................. 10-6 分配流路函数 ................................................................................................................ 10-6 分配流路命令 ......................................................................................................... 10-7 BPRINT 语句 .............................................................................................................. 10-7 CHAIN 语句 ........................................................................................................................... 10-7 CHR$ 函数 ............................................................................................................................... 10-7 清除命令 .......................................................................................................................... 10-7 时钟错误报警函数 .................................................................................................. 10-7 2000-OSM, C1 xiii 目录 (继续) Title Page 公用浮点数组 ....................................................................................................... 10-8 公用字符串组 ............................................................}
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